May 2007
Volume 48, Issue 13
Free
ARVO Annual Meeting Abstract  |   May 2007
Nuclear Magnetic Resonance Spectroscopy of Emulsified Oxane HD
Author Affiliations & Notes
  • P. J. Tomlins
    Ophthalmology, Birmingham and Midland Eye Centre, Birmingham, United Kingdom
  • M. G. L. Woodcock
    Ophthalmology, Birmingham and Midland Eye Centre, Birmingham, United Kingdom
  • N. Spencer
    School of Chemistry, University of Birmingham, Birmingham, United Kingdom
  • G. R. Kirkby
    Ophthalmology, Birmingham and Midland Eye Centre, Birmingham, United Kingdom
  • Footnotes
    Commercial Relationships P.J. Tomlins, None; M.G.L. Woodcock, None; N. Spencer, None; G.R. Kirkby, None.
  • Footnotes
    Support None.
Investigative Ophthalmology & Visual Science May 2007, Vol.48, 5751. doi:
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    • Get Citation

      P. J. Tomlins, M. G. L. Woodcock, N. Spencer, G. R. Kirkby; Nuclear Magnetic Resonance Spectroscopy of Emulsified Oxane HD. Invest. Ophthalmol. Vis. Sci. 2007;48(13):5751.

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      © ARVO (1962-2015); The Authors (2016-present)

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Abstract

Purpose:: Oxane HD® (Bausch and Lomb) is a mixture of 5700cs silicone oil and RMN-3 (a partially fluorinated olefin) which has a specific gravity greater than water, thereby enabling endotamponade of inferior retinal breaks. Droplets of emulsified oil were found in the anterior chamber of two patients with complex retinal detachments who had been treated with Oxane HD® We analysed samples removed from these two eyes in order to investigate the nature of the emulsified substance.

Methods:: Samples were dissolved in CDCl3 and, if necessary, dried using magnesium sulphate. Nuclear Magnetic Resonance (NMR) was used to compare these samples with the unused commercial product.

Results:: NMR analysis of the samples removed from anterior segment of both eyes show that they are composed mainly of silicone oil with only trace amounts of RMN-3. Samples taken from different areas of an unused syringe of Oxane HD® demonstrated varying concentrations of the RMN-3 compound within the silicone oil.

Conclusions:: Firstly, the mixture of RMN-3 and silicone oil is not homogenous either in vitro or in vivo. Secondly, emulsified oil found in the anterior chamber is composed almost entirely of silicone oil, containing only trace amounts of RMN-3.

Keywords: retinal detachment • vitreous substitutes • vitreoretinal surgery 
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