June 2022
Volume 63, Issue 7
Open Access
ARVO Annual Meeting Abstract  |   June 2022
Extended 24-h release of topical eye drop Dexamethasone formulation with single dose using silica microparticle-silica hydrogel composite technology
Author Affiliations & Notes
  • Frederic Dargelas
    DelSiTech Ltd, Turku, Finland
  • Minna Vaahtio
    DelSiTech Ltd, Turku, Finland
  • Mika Kaimainen
    DelSiTech Ltd, Turku, Finland
  • Hanumantha Rao Kamma
    Optifye Therapeutics AG, Switzerland
  • Janos Vaczi
    Optifye Therapeutics AG, Switzerland
  • Lasse Leino
    DelSiTech Ltd, Turku, Finland
  • Marcus Reay
    DelSiTech Ltd, Turku, Finland
  • Ossi Leppänen
    DelSiTech Ltd, Turku, Finland
  • Footnotes
    Commercial Relationships   Frederic Dargelas DelSiTech Ltd, Code E (Employment); Minna Vaahtio DelSiTech Ltd, Code E (Employment); Mika Kaimainen DelSiTech Ltd, Code E (Employment); Hanumantha Kamma Optifye Therapeutics AG, Code O (Owner); Janos Vaczi Optifye Therapeutics AG, Code E (Employment); Lasse Leino DelSiTech Ltd, Code E (Employment); Marcus Reay DelSiTech Ltd, Code E (Employment); Ossi Leppänen DelSiTech Ltd, Code E (Employment)
  • Footnotes
    Support  None
Investigative Ophthalmology & Visual Science June 2022, Vol.63, 2126 – F0142. doi:
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      Frederic Dargelas, Minna Vaahtio, Mika Kaimainen, Hanumantha Rao Kamma, Janos Vaczi, Lasse Leino, Marcus Reay, Ossi Leppänen; Extended 24-h release of topical eye drop Dexamethasone formulation with single dose using silica microparticle-silica hydrogel composite technology. Invest. Ophthalmol. Vis. Sci. 2022;63(7):2126 – F0142.

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      © ARVO (1962-2015); The Authors (2016-present)

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Abstract

Purpose : Topically administered therapies remain a standard of care for many ocular diseases. Frequent administration, as well as achieving stable therapeutic levels through the night poses a central challenge for effective maintenance of ocular health. As a result, the need to develop treatments with improved effective durations has gained significant attention. The purpose of this study was to investigate if a limited solubility therapeutic agent like dexamethasone (DEXA) could be efficiently encapsulated in Silica Matrix and demonstrate controlled release with a single 30 µL eye drop for 24 hours.

Methods : Two DEXA sustained release formulations, #09D and #12D) were tested. Dexamethasone was encapsulated in the Silica Matrix through sol-gel chemistry. New Zealand Rabbits were administered once with a single 30µL eyedrop in each eye. Tear samples were collected using a capillary up to 48 hours post dosing, and analyzed for DEXA by LC-MS/MS analysis from pooled left and right eye tear samples. In vitro DEXA and Si dissolutions were studied in sink condition and cumulative release as well as total dissolution and content was analyzed by spectrophotometry and HPLC. Intra ocular pressure (IOP) was monitored with Tonovet+ device.

Results : DEXA was successfully encapsulated in both silica microparticle-silica hydrogel formulations. In vivo pharmacokinetic data demonstrated extended controlled release of DEXA in rabbit tear fluid for 24 hours. Treatment was well tolerated and no changes in IOP were detected.

Conclusions : Efficient encapsulation of low solubility therapeutic agents like DEXA is possible by DelSiTechTM Silica Matrix technology ensuring extended release in-vivo for 24 hours.

This abstract was presented at the 2022 ARVO Annual Meeting, held in Denver, CO, May 1-4, 2022, and virtually.

 

 

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