Investigative Ophthalmology & Visual Science Cover Image for Volume 65, Issue 7
June 2024
Volume 65, Issue 7
Open Access
ARVO Annual Meeting Abstract  |   June 2024
Evaluating the Safety and Corneal Adherence of Topically Administered Novel Prodrug-Nanoparticles of Butyric Acid (BNP) in Mouse
Author Affiliations & Notes
  • Shashidhara Marulappa
    NanoScrips DBA, NutriForward, LLC, Carrollton, Texas, United States
  • Manas R Biswal
    Department of Pharmaceutical Sciences, University of South Florida Taneja College of Pharmacy, Tampa, Florida, United States
  • Radouil T Tzekov
    Department of Ophthalmology, University of South Florida Morsani College of Medicine, Tampa, Florida, United States
    Department of Pharmaceutical Sciences, University of South Florida Taneja College of Pharmacy, Tampa, Florida, United States
  • Alfred S Lewin
    Department of Molecular Genetics and Microbiology, University of Florida, Gainesville, Florida, United States
  • Footnotes
    Commercial Relationships   Shashidhara Marulappa NutriForward, LLC, Code O (Owner); Manas Biswal None; Radouil Tzekov NutriForward, LLC, Code C (Consultant/Contractor); Alfred Lewin NutriForward, LLC, Code C (Consultant/Contractor)
  • Footnotes
    Support  We would acknowledge the resources supported by grants from the National Eye Institute (NEI), R41EY034735 (M.R.B & S.M).
Investigative Ophthalmology & Visual Science June 2024, Vol.65, 3988. doi:
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      Shashidhara Marulappa, Manas R Biswal, Radouil T Tzekov, Alfred S Lewin; Evaluating the Safety and Corneal Adherence of Topically Administered Novel Prodrug-Nanoparticles of Butyric Acid (BNP) in Mouse. Invest. Ophthalmol. Vis. Sci. 2024;65(7):3988.

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      © ARVO (1962-2015); The Authors (2016-present)

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Abstract

Purpose : Overexpression of histone deacetylase (HDAC) and protein misfolding are implicated in many ophthalmic disorders including corneal scar formation, glaucoma, choroidal neovascularization (CNV) and retinal neurodegeneration. While currently available treatment options have improved the visual outcome, they are far from achieving a 100% success rate (non-responsiveness between 8 and 50% in CNV). An HDAC inhibitor as an alternative treatment option would be helpful as an independent treatment or adjunct to existing therapies. The purpose of our study was to test the safety and corneal adherence of novel version of a potent endogenous HDAC inhibitor: butyric acid (BA).

Methods : A co-polymer based, amphiphilic, self-assembling prodrug-nanoparticles of butyric acid (BNPs) were prepared. BNPs of size 40-50 nm were shown to release BA over 24-48 hrs. in serum. We tested the topical application (15.6 mg/mL) of TAMRA-labeled BNPs in wild type mice. A group of adult C57BL/6 mice (n=6) were dosed once a day for 3 days with TAMRA-labeled BNPs as a 10 μL eyedrop in one eye and the equivalent volume of PBS in the other eye as a control. Photographs of the cornea were taken before and at 3 hours after the last dose. After that, eyes were enucleated, cryopreserved and cryosectioned. Fluorescent imaging and histological evaluation of eyes was performed.

Results : All mice had clear and healthy-looking corneas at the beginning of the test and photographs showed no signs of inflammation or irritation. At the end of the dosing the ocular media were fully transparent, and the fundus had normal appearance in all mice. Histological evaluation showed no changes in the structure of the eye as a result of the dosing, incl. the retina and RPE. Clear fluorescence signal from TAMRA (at 579 nm) was detected 3 hours after the last dose on the corneal surface.

Conclusions : Topical administration of BNPs was found to be safe for ocular tissues in wild type mice after short-term dosing. BNPs appear to adhere to the corneal surface even after 3 hours of last application, which shows a potential for treatment of various anterior segment eye diseases. Research is ongoing to validate the efficacy of the proposed therapeutic agent.

This abstract was presented at the 2024 ARVO Annual Meeting, held in Seattle, WA, May 5-9, 2024.

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